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Introductory Mass Spectrometry

Stephen Shrader
€96.99
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Accurate Mass
advanced organic mass spectrometry applications
analytical chemistry techniques
assisted
Author_Stephen Shrader
Category=PNFS
Category=PNN
CH CH CH
chromatographic separation methods
desorption
electron impact fragmentation
Elemental Compositions
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exact
Exact Mass
Fragment Ions
GC-MS
GCMS Analysis
High Resolution Mass Measurements
High Resolution Mass Spectrometry
Highest Mass Peak
Intense Peak
ionization
ionization mechanisms
Isotope Peak
laser
LC-MS
Mass spectra
Mass Spectrometer
Mass spectrometry
Mass Spectrum
masses
matrix
McLafferty Rearrangement
Methyl Benzyl Ether
molecular
Molecular Ion
Molecular Ion Peak
Neutral Fragment
Odd Electron Ion
organic structure elucidation
Positive APCI
Positive ESI
Positive ESI Mass Spectrum
Quasi-molecular Ion
Simple Cleavage
spectral data interpretation
spectrometer
spectrum
Tropylium Ion

Product details

  • ISBN 9781466595842
  • Weight: 272g
  • Dimensions: 156 x 234mm
  • Publication Date: 12 Nov 2013
  • Publisher: Taylor & Francis Inc
  • Publication City/Country: US
  • Product Form: Paperback
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Description

Mass spectrometry has played an integral part in the study of organic molecular structures for more than 50 years, offering significant information from small amounts of sample. The mass spectrum produced by electron impact ionization presents a pattern of peaks that can often give definitive structural information about an unknown compound. Introductory Mass Spectrometry, Second Edition guides readers in the understanding and recognition of those patterns, discussing mass spectra in terms that are familiar to chemists. It provides a basis for chemists to interpret mass spectra to solve particular structural problems.

The Second Edition has been updated with modern techniques and data handling. Beginning with an introduction to the principles and instrumentation, it then sequentially explains the processes that occur in the mass spectrometer following ionization. The book is unique in the large number of mass spectra presented and provides examples of mass spectra from a wide variety of organic chemicals, concentrating on the relationships between fragmentation patterns, common chemical reactions, and chemical structures. The book also discusses mass spectra obtained with softer ionization techniques, which provide definitive information regarding molecular weights.

The text describes mass spectra produced by electron ionization, discussing how the spectral peak pattern relates to molecular structure. It details the use of high-resolution and accurate mass measurement to determine elemental composition of ions in order to identify unknown substances. The book also introduces some of the recent techniques that can be employed to extend the usefulness of mass spectrometry to high molecular weight substances and more polar substances. It includes examples and problems representing a cross section of organic chemistry to help readers integrate the principles presented.
About Stephen Shrader
Stephen Shrader , founder of Shrader Analytical and Consulting Laboratories, was among the early third-generation mass spectroscopists, starting in 1963. He is an internationally recognized expert in the use of mass spectrometry for structural elucidation and resolution of chemical problems in the petroleum, pharmaceutical, environmental, and polymer fields. His work has included periods in academia, the pharmaceutical industry, and a long stint as a consultant to the overall chemical industry. Throughout his 40-plus-year career, he has shared his experiences and knowledge of mass spectrometry via numerous seminars and classes. He has also been instrumental in developing a set of software tools called TSS Unity for displaying, printing, and evaluating mass spectral data for the purpose of solving chemical problems.

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